On thermal runaway and local endothermic/exothermic reactions during flash sintering of ceramic nanoparticles
نویسندگان
چکیده
منابع مشابه
Thermal runaway, flash sintering and asymmetrical microstructural development of ZnO and ZnO–Bi2O3 under direct currents
DC flash sintering of both pure and 0.5 mol.% Bi2O3-doped ZnO at a relatively high activating field of 300 V/cm has been investigated. It is demonstrated that even high-purity ZnO single crystals can “flash” at 870 C. In comparison, flash sintering occurs at a substantially lower onset temperature of 550 C in ZnO powder specimens, indicating the important roles of surfaces and/or grain boundari...
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Recently, local melting of the particle surfaces confirmed the formation of spark and plasma during spark plasma sintering, which explains the rapid densification mechanism via liquid. A model for rapid densification of flash sintered ceramics by liquid film capillary was presented, where liquid film forms by local melting at the particle contacts, due to Joule heating followed by thermal runaw...
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The deposition of nano-size copper particles was carried out by means of ink-jet printing on the ceramic substrate (silicon and faience) using Nd +3 :YAG laser. Glycerin and aqueous based nano copper inks were prepared and were inkjetted in this study. The sintered copper film had a grainy structure with neck-like junctions. The microstructure and soldering properties were examined using XRD, S...
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Flash sintering as a new sintering method for sintering of ceramic materials has been studied and effect of various parameter such as flash current density, time of flash and contact paste on properties of flash sintered 8YSZ samples has been investigated. Results showed it is possible to achieve high density in shorter time and lower temperature than conventional sintering methods. Samples cou...
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Using ZnO as a model system, the densification mechanisms of flash sintering are investigated. Controlled experiments via limiting the maximum current or the effective ramp rate suggest that both the maximum specimen temperature and the high heating rate (on the order of 200 C/s) are essential for the rapid densification during the flash sintering. Moreover, benchmarking rapid thermal annealing...
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ژورنال
عنوان ژورنال: Journal of Materials Science
سال: 2018
ISSN: 0022-2461,1573-4803
DOI: 10.1007/s10853-018-2040-y